Dataset: Fall 2011 - Porewater Samples
Deployment: ESAS_Fall_2011

Fall 2011 - Porewater Samples

Lead Principal Investigator:

Samantha B. Joye (University of Georgia, UGA)

Co-Principal Investigator:

Christof Meile (University of Georgia, UGA)

Vladimir Samarkin (University of Georgia, UGA)

Contact:

Samantha B. Joye (University of Georgia, UGA)

BCO-DMO Data Manager:

Stephen R. Gegg (Woods Hole Oceanographic Institution, WHOI BCO-DMO)

Project:

Collaborative Research: Degrading offshore permafrost as a source of methane on the East Siberian Arctic Shelf (East Siberian Arctic Shelf)

Current State:

Preliminary and in progress

Version:

20 April 2016

Version Date:

2016-04-20

Data URL:

https://www.bco-dmo.org/dataset-deployment/644545/data

Expand/Collapse All

Description

Fall 2011 - Porewater Samples

Methods & Sampling

Dataset acquisition description

Fall 2011 - Porewater Samples

Porewater samples collected for: Analytical Method Instrument Method Reference
Dissolved Organic Carbon High temperature combustion Shimadzu TOC-V http://www.pangaea.de/Projects/JGOFS/Methods/chap16.html;
Total Dissolved Nitrogen High temperature combustion/Chemiluminescence Shimadzu TOC-V with TN Unit Pan et al., Simultaneous Determination of Dissolved Organic Carbon and Total Dissolved Nitrogen on a Coupled High-Temperature Combustion Total Organic Carbon-Nitrogen Chemiluminescence Detection (HTC TOC-NCD) System. Journal of Automated Methods & Management in Chemistry, 2005 (2005), no. 4, 240–246
Total Dissolved Phosphorus Spectrophotometry Shimadzu UV-1601 Solorzano, L., and Sharp, J. H. 1980. Determination of total dissolved phosphorus and particulate phosphorus in natural waters. Limnol. Oceanogr. 25: 754-758.
NOx (Nitrate + Nitrite) Flow Injection Autoanalyzer Lachat Instruments FIA+ 8000 Series Lachat Instruments FIA 8000 Autoanalyzer Method 31-107-04-1-A
Nitrite Flow Injection Autoanalyzer Lachat Instruments FIA+ 8000 Series Lachat Instruments FIA 8000 Autoanalyzer Method 31-107-04-1-A
Orthophosphate Flow Injection Autoanalyzer Lachat Instruments FIA+ 8000 Series Lachat Instruments FIA 8000 Autoanalyzer Method 31-115-01-1-H
Reactive Silicate Flow Injection Autoanalyzer Lachat Instruments FIA+ 8000 Series Lachat Instruments FIA 8000 Autoanalyzer Method 31-114-27-1-D
Ammonium Spectrophotometry Shimadzu UV-1601 Solorzano, L. 1969. Determination of ammonia in natural waters by the phenolhypochlorite method. Limnol. Oceanogr. 14: 799-801
Anions (Sulfate + Chloride) Ion Chromatography DIONEX ICS-2000 DIONEX Application Note 154: Determination of Inorganic Anions in Environmental Waters Using a Hydroxide-Selective Column.
Anaerobic Methane Oxidation Sediment incubations with 14CH4 Scintillation Counter Orcutt, B., et al. 2005. Molecular biogeochemistry of sulfate reduction, methanogenesis and the anaerobic oxidation of methane at Gulf of Mexico methane seeps. GCA Vol. 69, No. 17, pp. 4267–4281

References:
Joye SB, Bowles M.W., Samarkin V.A., Hunter K.S., Niemann H.. 2010. Biogeochemical signatures and microbial activity of different cold seep habitats along the Gulf of Mexico lower slope. Deep Sea Research. 10:doi:10.1016/j.dsr2.2010.06.001.

Joye SB, MacDonald I.R., Leifer I., Asper V.. 2011. Magnitude and oxidation potential of hydrocarbon gases released from the BP blowout. Nature Geoscience. 4:160-164.

Orcutt B.N., Samarkin V., Boetius A., Elvert M., Joye SB. 2005. Molecular biogeochemistry of sulfate reduction, methanogenesis and the anaerobic oxidation of methane at Gulf of Mexico methane seeps. Geochimica et Cosmochimica Acta. 69:4267-4281.

Data Processing Description

Dataset Processing Description

BCO-DMO Processing Notes
- Generated from original file "00908788_Joye_Fall-2011_Data-Summary.xlsx", Sheet: "Porewater Data" contributed by Samantha Joye
- Parameter names edited to conform to BCO-DMO naming convention found at Choosing Parameter Name
- "nd" (no data) inserted into blank cells
- blank rows removed
- "B.D.L." converted to "BDL" (periods removed) to avoid potential data errors downstream
- "N.S." converted to "NS" (periods removed) to avoid potential data errors downstream and for consistency

More information about this dataset deployment

Funding

Award Number	Funding Source
PLR-0908788	NSF Division of Polar Programs

Instruments

Drill Core

Supplied Description:

Instrument Type

Generic Name: Drill Core

Generic Description:

A core drill is a drill specifically designed to remove a cylinder of material, much like a hole saw. The material left inside the drill bit is referred to as the core.

Core drills are used frequently in mineral exploration where the coring may be several hundred to several thousand feet in length. The core samples are recovered and examined by geologists for mineral percentages and stratigraphic contact points. This gives exploration companies the information necessary to begin or abandon mining operations in a particular area.

Flow Injection Analyzer

Supplied Name: Lachat Instruments FIA+ 8000 Series

Supplied Description:

Porewater samples collected for:
NOx (Nitrate + Nitrite)
Nitrite
Orthophosphate
Reactive Silicate

Analytical Method: Flow Injection Autoanalyzer

Instrument: Lachat Instruments FIA+ 8000 Series

Method Reference(s):
Lachat Instruments FIA 8000 Autoanalyzer Method 31-107-04-1-A
Lachat Instruments FIA 8000 Autoanalyzer Method 31-115-01-1-H
Lachat Instruments FIA 8000 Autoanalyzer Method 31-114-27-1-D

Instrument Type

Generic Name: Flow Injection Analyzer

Acronym: FIA

Community Identifier: http://vocab.nerc.ac.uk/collection/L05/current/LAB36/

Generic Description:

An instrument that performs flow injection analysis. Flow injection analysis (FIA) is an approach to chemical analysis that is accomplished by injecting a plug of sample into a flowing carrier stream. FIA is an automated method in which a sample is injected into a continuous flow of a carrier solution that mixes with other continuously flowing solutions before reaching a detector. Precision is dramatically increased when FIA is used instead of manual injections and as a result very specific FIA systems have been developed for a wide array of analytical techniques.

Gravity Corer

Supplied Name: Gravity Core

Supplied Description:

Instrument Type

Generic Name: Gravity Corer

Community Identifier: http://vocab.nerc.ac.uk/collection/L05/current/51/

Generic Description:

The gravity corer allows researchers to sample sediment layers at the bottom of lakes or oceans. The coring device is deployed from the ship and gravity carries it to the seafloor. (http://www.whoi.edu/instruments/viewInstrument.do?id=1079).

Ion Chromatograph

Supplied Name: DIONEX ICS-2000

Supplied Description:

Porewater samples collected for: Anions (Sulfate + Chloride)

Analytical Method: Ion Chromatography

Instrument: DIONEX ICS-2000

Method Reference: DIONEX Application Note 154: Determination of Inorganic Anions in Environmental Waters Using a Hydroxide-Selective Column

Instrument Type

Generic Name: Ion Chromatograph

Generic Description:

Ion chromatography is a form of liquid chromatography that measures concentrations of ionic species by separating them based on their interaction with a resin. Ionic species separate differently depending on species type and size. Ion chromatographs are able to measure concentrations of major anions, such as fluoride, chloride, nitrate, nitrite, and sulfate, as well as major cations such as lithium, sodium, ammonium, potassium, calcium, and magnesium in the parts-per-billion (ppb) range. (from http://serc.carleton.edu/microbelife/research_methods/biogeochemical/ic.html)

Liquid Scintillation Counter

Supplied Name: Scintillation Counter

Supplied Description:

Porewater samples collected for: Anaerobic Methane Oxidation

Analytical Method: Sediment incubations with 14CH4

Instrument: Scintillation Counter

Method Reference: Orcutt, B., et al. 2005. Molecular biogeochemistry of sulfate reduction, methanogenesis and the anaerobic oxidation of methane at Gulf of Mexico methane seeps. GCA Vol. 69, No. 17, pp. 4267–4281

Instrument Type

Generic Name: Liquid Scintillation Counter

Acronym: LSC

Community Identifier: http://vocab.nerc.ac.uk/collection/L05/current/LAB21/

Generic Description:

Liquid scintillation counting is an analytical technique which is defined by the incorporation of the radiolabeled analyte into uniform distribution with a liquid chemical medium capable of converting the kinetic energy of nuclear emissions into light energy. Although the liquid scintillation counter is a sophisticated laboratory counting system used the quantify the activity of particulate emitting (ß and a) radioactive samples, it can also detect the auger electrons emitted from 51Cr and 125I samples.

Liquid scintillation counters are instruments assaying alpha and beta radiation by quantitative detection of visible light produced by the passage of rays or particles through a suitable scintillant incorporated into the sample.

Shimadzu TOC-V Analyzer

Supplied Name: Shimadzu TOC-V

Supplied Description:

Porewater samples collected for: Dissolved Organic Carbon

Analytical Method: High temperature combustion

Instrument: Shimadzu TOC-V

Method Reference: http://www.pangaea.de/Projects/JGOFS/Methods/chap16.html

Instrument Type

Generic Name: Shimadzu TOC-V Analyzer

Acronym: Shimadzu TOC-V

Community Identifier: http://onto.nerc.ac.uk/CAST/124

Generic Description:

A Shimadzu TOC-V Analyzer measures DOC by high temperature combustion method.

Shimadzu TOC-V Analyzer

Supplied Name: Shimadzu TOC-V with TN Unit

Supplied Description:

Porewater samples collected for: Total Dissolved Nitrogen

Analytical Method: High temperature combustion/Chemiluminescence

Instrument: Shimadzu TOC-V with TN Unit

Method Reference: Pan et al., Simultaneous Determination of Dissolved Organic Carbon and Total Dissolved Nitrogen on a Coupled High-Temperature Combustion Total Organic Carbon-Nitrogen Chemiluminescence Detection (HTC TOC-NCD) System. Journal of Automated Methods & Management in Chemistry, 2005 (2005), no. 4, 240–246

Instrument Type

Generic Name: Shimadzu TOC-V Analyzer

Acronym: Shimadzu TOC-V

Community Identifier: http://onto.nerc.ac.uk/CAST/124

Generic Description:

A Shimadzu TOC-V Analyzer measures DOC by high temperature combustion method.

UV Spectrophotometer-Shimadzu

Supplied Name: Shimadzu UV-1601

Supplied Description:

Porewater samples collected for: Total Dissolved Phosphorus and Ammonium

Analytical Method: Spectrophotometry

Instrument: Shimadzu UV-1601

Method Reference:
Solorzano, L., and Sharp, J. H. 1980. Determination of total dissolved phosphorus and particulate phosphorus in natural waters. Limnol. Oceanogr. 25: 754-758.
Solorzano, L. 1969. Determination of ammonia in natural waters by the phenolhypochlorite method. Limnol. Oceanogr. 14: 799-801

Instrument Type

Generic Name: UV Spectrophotometer-Shimadzu

Community Identifier: http://vocab.nerc.ac.uk/collection/L05/current/LAB20/

Generic Description:

The Shimadzu UV Spectrophotometer is manufactured by Shimadzu Scientific Instruments (ssi.shimadzu.com). Shimadzu manufacturers several models of spectrophotometer; refer to dataset for make/model information.

Parameters

Supplied Name	Supplied description	Supplied Units	Standard Name
Porewater_ID	Porewater ID	dimensionless	sample
Station	Station	dimensionless	station
Date	Date	text	date
Latitude	Station latitude (South is negative)	decimal degrees	lat
Longitude	Station longitude (West is negative)	decimal degrees	lon
Water_Depth	Water_Depth	meters	depth
Depth_Range	Depth_Range	cbsf	depth_range
DOC	DOC	uM	DOC
TDN	TDN	uM	TDN
NOx	NOx (Nitrate + Nitrite)	uM	NO3_NO2_pw
NO2	NO2	uM	NO2
NH4	NH4	uM	NH4
TDP	TDP	uM	TDP
PO4	PO4	uM	PO4
Si	Si	uM	Si
SO4	SO4	mM	SO4
Cl	Cl	mM	no_bcodmo_term
Anaerobic_Methane_Oxidation_Turnover_Constant_k	Anaerobic Methane Oxidation Turnover Constant k	1/d	no_bcodmo_term

Database

Contribute Data

Dataset: Fall 2011 - Porewater Samples
Deployment: ESAS_Fall_2011

Dataset acquisition description

Dataset Processing Description

Database

Contribute Data

Dataset: Fall 2011 - Porewater SamplesDeployment: ESAS_Fall_2011

Dataset acquisition description

Dataset Processing Description

Dataset: Fall 2011 - Porewater Samples
Deployment: ESAS_Fall_2011